188290-36-0合成路线 (共 917 条)
反应条件
n-butyllithium Yield given. Multistep reaction;
参考文献
Verkruijsse, H. D.; Brandsma, L.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 95 - 98
反应条件
tin(IV) chloride; 1,2-dichloro-ethane
参考文献
Buess; Kharasch
Journal of the American Chemical Society, 1959 , vol. 72, p. 3529,3530, 3531
反应条件
tin(IV) chloride in dichloromethane; benzene T=0°C; 1 h;
参考文献
Choi, Jung Hei; Son, Kyung-In; Kim, Taehee; Kim, Kyungkon; Ohkubo, Kei; Fukuzumi, Shunichi
Journal of Materials Chemistry, 2010 , vol. 20, # 3 p. 475 - 482
反应条件
thionyl chloride; tin(IV) chloride 1.) CH2Cl2, reflux, 3 h, 2.) CH2Cl2, -5 deg C to 5 deg C; Yield given. Multistep reaction;
参考文献
Wierzbicki, Michel; Boussard, Marie-Francoise; Sauveur, Frederic; Kirsch, Gilbert; Sabatini, Massimo; Lesur, Christophe; Trodjman, Charles; Bonnet, Jacqueline
Arzneimittel-Forschung/Drug Research, 1998 , vol. 48, # 8 p. 840 - 849
反应条件
NISacc T=20°C; Ionic liquidDarkness;
参考文献
Bailey, Lindsey; Handy, Scott T.
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2413 - 2414
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; ZnCl2*TMEDA in tetrahydrofuran; hexane T=0 - 20°C; Inert atmosphere; 2: With iodine in tetrahydrofuran; hexane Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 27 p. 8191 - 8201
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate; zinc(II) chloride in acetic acid T=70°C; 24 h; Yield given. Yields of byproduct given;
参考文献
D'Auria; Mauriello
Synthesis, 1995 , # 3 p. 248 - 250
参考文献
Datta; Chatterjee
Journal of the American Chemical Society, 1917 , vol. 39, p. 437
参考文献
Steinkopf
Justus Liebigs Annalen der Chemie, 1923 , vol. 430, p. 104
参考文献
Meyer,V.; Kreis
Chemische Berichte, 1884 , vol. 17, p. 1561
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Thyssen
Journal fuer Praktische Chemie (Leipzig), 1902 , vol. <2> 65, p. 5