188290-36-0合成路线 （共 917 条）
反应条件
T=25°C; Irradiation; Product distributionKinetics;
参考文献
Herrera, Olga S.; Nieto, Jorge D.; Lane, Silvia I.; Oexler, Elena V.
Canadian Journal of Chemistry, 2003 , vol. 81, # 12 p. 1477 - 1481
反应条件
1: bromodifluoromethyl phenyl sulphide With titanium tetrachloride in dichloromethane T=20°C; Friedel Crafts type alkylation; 0.25 h; Inert atmosphere; 2: thiophene in dichloromethane T=20°C; Friedel Crafts type alkylation; 2 h; Inert atmosphere;
参考文献
Kuhakarn, Chutima; Surapanich, Nakin; Kamtonwong, Siriporn; Pohmakotr, Manat; Reutrakul, Vichai
European Journal of Organic Chemistry, 2011 , # 29 p. 5911 - 5918
反应条件
T=350°C; P=51485.6 Torr; Hydrogenation;
参考文献
Pines; Postl
Journal of the American Chemical Society, 1957 , vol. 79, p. 1769
反应条件
hydrogenchloride T=10°C; 1 h;
参考文献
Waser, Jerome; Gaspar, Boris; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2006 , vol. 128, # 35 p. 11693 - 11712
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2: 1-bromo-decane in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Pu, Shouzhi; Zhu, Shengsheng; Rao, Yi; Liu, Gang; Wei, Huizhen
Journal of Molecular Structure, 2009 , vol. 921, # 1-3 p. 89 - 100
反应条件
1: thiophene With n-butyllithium in hexane T=-78°C; 1 h; 2: n-decyl iodide in hexane T=-78 - 20°C;
参考文献
Wilson, Paul; Lacey, David; Sharma, Sanjay; Worthington, Brenda
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 368, p. 279 - 292
反应条件
1: thiophene With n-butyllithium in diethyl ether; hexane T=20°C; 1 h; 2: dimethylmono-chlorosilane in diethyl ether; hexane T=-78 - 20°C; 3 h; Further stages.;
参考文献
Vitale, Maxime; Prestat, Guillaume; Lopes, David; Madec, David; Kammerer, Claire; Poli, Giovanni; Girnita, Leonard
Journal of Organic Chemistry, 2008 , vol. 73, # 15 p. 5795 - 5805
反应条件
palladium diacetate; caesium carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl-formamide T=100°C; 2 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
反应条件
tetrahydrofuran; lithium T=-196.15°C;
参考文献
Mendoza, Oscar; Rehmann, Franz-Josef K.; Cuffe, Laurence P.; Tacke, Matthias
European Journal of Inorganic Chemistry, 2004 , # 22 p. 4525 - 4532
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Bagnoli, Luana; Marini, Francesca; Temperini, Andrea; Tomassini, Cristina; Santi, Claudio
Tetrahedron, 2000 , vol. 56, # 20 p. 3255 - 3260
