188290-36-0 合成路线 (共 917 条)
55591-23-6 1,1,2,2,3,3,4,4,5,5,6,6,6-十三氟己烷-1-磺酰氯
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反应条件
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) in pentane T=120°C; 24 h;
参考文献
Kamigata, Nobumasa; Ohtsuka, Takeshi; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 96, # 1-4 p. 491 - 492
反应条件
sodium dithionite; sodium hydrogencarbonate in dimethyl sulfoxide T=75°C; 8 h; Title compound not separated from byproducts;
参考文献
Huang; Long; Chen
Journal of Fluorine Chemistry, 2001 , vol. 111, # 2 p. 107 - 113
反应条件
tin(IV) chloride in benzene T=30°C; Friedel-Crafts acylation; 3 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
PPA T=60 - 80°C; Acylation; Friedel-Crafts acylation; 2 h;
参考文献
Renault, Olivier; Dallemagne, Patrick; Rault, Sylvain
Organic Preparations and Procedures International, 1999 , vol. 31, # 3 p. 324 - 328
反应条件
zinc dibromide in dichloromethane T=90°C; 12 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Croatica Chemica Acta, 2004 , vol. 77, # 1-2 p. 175 - 178
反应条件
PPA T=60 - 80°C; Acylation; Friedel-Crafts acylation; 2 h;
参考文献
Renault, Olivier; Dallemagne, Patrick; Rault, Sylvain
Organic Preparations and Procedures International, 1999 , vol. 31, # 3 p. 324 - 328
反应条件
sodium dithionite; sodium hydrogencarbonate in dimethyl sulfoxide T=75°C; 8 h; Title compound not separated from byproducts;
参考文献
Huang; Long; Chen
Journal of Fluorine Chemistry, 2001 , vol. 111, # 2 p. 107 - 113
反应条件
n-butyllithium Multistep reaction. Title compound not separated from byproducts;
参考文献
Tempkin, Orin; Blacklock, Thomas J.; Burke, J. Andrew; Anastasia, Maria
Tetrahedron Asymmetry, 1996 , vol. 7, # 9 p. 2721 - 2724
反应条件
biscyclopentadienyliron(II); hydrogen; iron in gaseous matrix catalyst precursor: ferrocene; ferrocene evapn., mixing with benzene, thiophene and H2; temp. 1100-1200°C, 1-30 min; according to M. Endo, M. Shikata, Ohyo Butsuri 54 (1985) 507; electron microscopy;
参考文献
Chemical Physics Letters, , vol. 289, # 5-6 p. 602 - 610
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=130°C; 20 h; Inert atmosphere;
参考文献
Bensaid, Souhila; Roger, Julien; Beydoun, Kassem; Roy, David; Doucet, Henri
Synthetic Communications, 2011 , vol. 41, # 23 p. 3524 - 3531