188290-36-0合成路线 （共 917 条）
反应条件
sodium hydroxide; magnesium sulfate
参考文献
Gomberg; Bachmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2343
Journal of the American Chemical Society, 1927 , vol. 49, p. 250
反应条件
1: p-aminobenzonitrile With tetrafluoroboric acid; sodium nitrite in water T=0°C; 2: thiophene With Eosin in dimethyl sulfoxide T=20°C; 16 h; Irradiation;
参考文献
Hari, Durga Prasad; Schroll, Peter; Koenig, Burkhard
Journal of the American Chemical Society, 2012 , vol. 134, # 6 p. 2958 - 2961
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=130°C; 20 h; Inert atmosphere;
参考文献
Bensaid, Souhila; Roger, Julien; Beydoun, Kassem; Roy, David; Doucet, Henri
Synthetic Communications, 2011 , vol. 41, # 23 p. 3524 - 3531
参考文献
Pines et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1563,1567
参考文献
Caesar
Journal of the American Chemical Society, 1948 , vol. 70, p. 2623
反应条件
potassium tetrachloropalladate in ethanol; water 24 h; Ambient temperature;
参考文献
Journal of Organometallic Chemistry, , vol. 406, # 3 p. C29 - C32
反应条件
n-butyllithium; tributyltin chloride; tetrakis(triphenylphosphine) palladium(0) 1.) THF, RT, overnight, 2.) toluene, reflux, 18 h; Yield given. Multistep reaction;
参考文献
Yui, Koji; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 5 p. 1539 - 1546
反应条件
in ethanol; water byproducts: tetrathiophene; at room temp. for 24 h under N2; concn.; extn. (CHCl3); combined CHCl3-extracts were concd.; chromy. (n-hexane; silica gel); NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 406, # 3 p. C29 - C32
反应条件
palladium diacetate; potassium carbonate; tri-cyclo-hexyl-phosphine; 2,2,2-trimethylacetic acid in N,N-dimethyl-formamide T=180°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Baghbanzadeh, Mostafa; Pilger, Christian; Oliver Kappe
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 8138 - 8142
反应条件
manganese triacetate Heating;
参考文献
Demir, Ayhan S.; Reis, Oemer; Emrullahoglu, Mustafa
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 578 - 580
