188290-36-0合成路线 (共 917 条)
反应条件
T=130°C; 1 h; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 27, # 9 p. 1105 - 1108
反应条件
MechanismProduct distribution;
参考文献
Tetrahedron Letters, , vol. 27, # 9 p. 1105 - 1108
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=130°C; 20 h; Inert atmosphere;
参考文献
Bensaid, Souhila; Roger, Julien; Beydoun, Kassem; Roy, David; Doucet, Henri
Synthetic Communications, 2011 , vol. 41, # 23 p. 3524 - 3531
反应条件
manganese triacetate Heating;
参考文献
Demir, Ayhan S.; Reis, Oemer; Emrullahoglu, Mustafa
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 578 - 580
反应条件
Tl(OCOCF3)3 in trifluoroacetic acid Irradiation;
参考文献
Fabian, J.; Mayer, R.; Bleisch, S.; Zahradnik, R.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 107 - 118
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78 - -20°C; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C;
参考文献
Kim, Dae-Sik; Kyo, Han Ahn
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6831 - 6834
反应条件
n-butyllithium in tetrahydrofuran thiophene and n-BuLi in hexane mixed in THF at 0°C under N2; B(OEt)2 added dropwise at -70°C; temp. raised to room temp. and aq. H2SO4 added followed CH2Cl2; org. layer extd. with aq. NaOH; to aq. layer added aq. HCl and compd. extd. with dichloromethane;
参考文献
Dufresne, Stephane; Hanan, Garry S.; Skene
Journal of Physical Chemistry B, 2007 , vol. 111, # 39 p. 11407 - 11418
反应条件
potassium carbonate in acetonitrile 3 h; Irradiation;
参考文献
Tetrahedron, , vol. 56, # 47 p. 9383 - 9389
反应条件
1: With mercury(II) trifluoroacetate in benzene T=0°C; 0.25 h; 2: With triethylamine; palladium dichloride in benzene T=0°C; 0.25 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7523 - 7525
反应条件
1: With mercury(II) trifluoroacetate in benzene T=0°C; 0.25 h; 2: With triethylamine; palladium dichloride in benzene T=0°C; 0.25 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7523 - 7525