188290-36-0合成路线 （共 917 条）
反应条件
Yield given. Multistep reaction;
参考文献
Kagan, Jacques; Arora, Sudershan K.
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4043 - 4046
反应条件
zinc oxide T=25 - 30°C; Friedel-Crafts Acylation; 0.166667 h; regioselective reaction;
参考文献
More, Parmeshwar E.; Bandgar, Babasaheb P.; Kamble, Vinod T.
Catalysis Communications, 2012 , vol. 27, p. 30 - 32
反应条件
iron(III) chloride in carbon disulfide 3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
aluminium trichloride; nitromethane in carbon disulfide 3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
aluminium trichloride in carbon disulfide 3 h; Ambient temperatureother catalyst; Product distribution;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
1: thiophene With N-tetramethylpiperidine magnesium chloride; lithium chloride in tetrahydrofuran T=25°C; 24 h; 2: N,N-dimethyl-formamide in tetrahydrofuran T=-30°C;
参考文献
Krasovskiy, Arkady; Krasovskaya, Valeria; Knochel, Paul
Angewandte Chemie - International Edition, 2006 , vol. 45, # 18 p. 2958 - 2961
反应条件
n-butyllithium in tetrahydrofuran; hexane T=0°C; 2 h;
参考文献
H. LUNDBECK A/S
Patent: WO2004/58739 A1, 2004 ;
Location in patent: Page 45; 57 ;
反应条件
sulfuric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile T=80°C; 5 h;
参考文献
Branytska, Oiena; Neumann, Ronny
Synlett, 2004 , # 9 p. 1575 - 1576
反应条件
1: thiophene With chloromagnesium diisopropylamide in tetrahydrofuran T=20°C; 24 h; 2: 1-piperidinecarboxaldehyde in tetrahydrofuran T=20°C; 27 h; Further stages.;
参考文献
Shilai, Manabu; Kondo, Yoshinori; Sakamoto, Takao
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 442 - 444
反应条件
aluminium trichloride in chlorobenzene T=40°C; Formylation; 0.1 h;
参考文献
Kantlehner, Willi; Vettel, Markus; Gissel, Alexander; Haug, Erwin; Ziegler, Georg; Ciesielski, Michael; Scherr, Oliver; Haas, Richard
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 3 p. 297 - 310
