188290-36-0合成路线 (共 917 条)
参考文献
Karrer; Rebmann; Zeller
Helvetica Chimica Acta, 1920 , vol. 3, p. 266
参考文献
Steinkopf; Ohse
Justus Liebigs Annalen der Chemie, 1924 , vol. 437, p. 19
反应条件
silver hexafluoroantimonate; [PtCl2(PhCN)2] in dichloromethane Friedel-Crafts acylation; Heating;
参考文献
Organic Letters, , vol. 3, # 3 p. 417 - 420
反应条件
polystyrene supported aluminium triflate T=20°C; Friedel-Crafts acylation; 2.1 h; Neat (no solvent); regioselective reaction;
参考文献
Bulletin of the Korean Chemical Society, , vol. 31, # 11 p. 3156 - 3158
反应条件
1: benzoic acid t-butyl ester With indium tribromide; dimethylmono-chlorosilane in 1,2-dichloro-ethane T=20°C; 2 h; Inert atmosphere; 2: thiophene in 1,2-dichloro-ethane T=90°C; Friedel Crafts acylation; 10 h; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 73, # 23 p. 9465 - 9468
反应条件
2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate in dichloromethane T=20°C; Friedel-Crafts reaction; 1 h;
参考文献
Chemistry Letters, , vol. 37, # 6 p. 650 - 651
反应条件
trifluoromethanesulfonic acid 2-pyridinyl ester; trifluoroacetic acid 4 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 455 - 460
反应条件
HZSM-5 in 1,2-dichloro-ethane Heating;
参考文献
Tetrahedron Letters, , vol. 35, # 16 p. 2601 - 2602
反应条件
in dichloromethane T=20°C; 0.7 h;
参考文献
Chemische Berichte, , vol. 114, # 3 p. 926 - 936
反应条件
1: thiophene With n-butyllithium; CuCl2*TMEDA; 2,2,6,6-tetramethylpiperidinyl-lithium in hexanes; dimethylsulfide; diethyl ether T=20°C; 2 h; Inert atmosphere; 2: benzoyl chloride in hexanes; dimethylsulfide; diethyl ether T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 37 p. 10405 - 10416