188290-36-0合成路线 （共 917 条）
反应条件
anhydrous iron chloride; silver hexafluoroantimonate in 1,2-dichloro-ethane T=80°C; Friedel-Crafts Alkylation; 24 h; Inert atmosphere; Overall yield = 65 percent; Overall yield = 107.2 mg; regioselective reaction;
参考文献
Jefferies, Latisha R.; Cook, Silas P.
Organic Letters, 2014 , vol. 16, # 7 p. 2026 - 2029
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5099,5101
反应条件
1: With mercury(II) trifluoroacetate in benzene T=0°C; 0.25 h; 2: With triethylamine; palladium dichloride in benzene T=0°C; 0.25 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7523 - 7525
反应条件
ethylaluminum dichloride in dichloromethane T=0°C; 2 h; Inert atmosphere;
参考文献
Uenver, Halil; Biyikoglu, Mutluhan; Bulut, Adnan
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8772 - 8774
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=16 - 20°C; 4.5 h; Yields of byproduct given;
参考文献
Merz; Ellinger
Synthesis, 1991 , # 6 p. 462 - 464
反应条件
AlCl3, aluminium chloride in dichloromethane T=40°C; 12 h;
参考文献
Smirnov; Afanas'Ev; Belen'kii
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 10 p. 1199 - 1207
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 3 h;
参考文献
Smirnov; Afanas'Ev; Belen'kii
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 10 p. 1199 - 1207
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 3 h;
参考文献
Smirnov; Afanas'Ev; Belen'kii
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 10 p. 1199 - 1207
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 1 h; 2: 1-bromo-butane in tetrahydrofuran; hexane T=-40 - 20°C;
参考文献
Van Breemen, Albert J. J. M.; Herwig, Peter T.; Chlon, Ceciel H. T.; Sweelssen, Joergen; Schoo, Herman F. M.; Setayesh, Sepas; Hardeman, Willie M.; Martin, Christian A.; De Leeuw, Dago M.; Valeton, Josue J. P.; Bastiaansen, Cees W. M.; Broer, Dirk J.; Popa-Merticaru, Andreea R.; Meskers, Stefan C. J.
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2336 - 2345
反应条件
phosphoric acid T=120°C; Hydrieren der bei 99.5grad/48 Torr und 97grad/39 Torr siedenden Anteile des Reaktionsprodukts an Palladium/Aluminiumoxid bei 80-100grad/100 at;
参考文献
Pines et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5173
