188290-36-0合成路线 （共 917 条）
反应条件
aluminium trichloride in dichloromethane T=-70°C; 1 h; ratio of th σ-complexes, effect of time and temperature and other halides was investigated; MechanismProduct distribution;
参考文献
Belen'kii, L. I.; Yakubov, A. P.
Tetrahedron, 1984 , vol. 40, # 13 p. 2471 - 2477
反应条件
oxygen; trimethylamine Irradiationvariation of the total pressure, variation of the concentration of NMe3;
参考文献
Margonelli, Andrea; Speranza, Maurizio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 1491 - 1498
参考文献
Sy et al.
Journal of the Chemical Society, 1954 , p. 1975,1977
反应条件
methanesulfonic acid T=30°C; 5.5 h;
参考文献
Bioorganic and medicinal chemistry letters, , vol. 12, # 17 p. 2317 - 2320
反应条件
in acetonitrile 5 h; Irradiation;
参考文献
Hatjiarapoglou, Lazaros; Varvoglis, Anastasios
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1599 - 1600
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=-50.16 - -40.16°C; 1 h; 2: [2,2']bipyridinyl in tetrahydrofuran; hexane T=20°C; 12 h;
参考文献
Bozic-Weber, Biljana; Constable, Edwin C.; Housecroft, Catherine E.; Kopecky, Peter; Neuburger, Markus; Zampese, Jennifer A.
Dalton Transactions, 2011 , vol. 40, # 46 p. 12584 - 12594
反应条件
aluminium trichloride 1.) nitromethane, 5-12 deg C;2.) room temperature, 10 h; Yield given. Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 4 p. 449 - 458
反应条件
1: thiophene With n-butyllithium in hexanes; diethyl ether T=-78 - 0°C; 1 h; 2: copper (I) cyanide in hexanes; diethyl ether T=-78 - 20°C; 0.5 - 1 h;
参考文献
ALLERGAN, INC.
Patent: WO2006/63179 A1, 2006 ;
Location in patent: Page/Page column 38-39; 48-49 ;
WO 2006/063179 A1
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran T=-40°C; 0.666667 h; 2: With zinc(II) chloride in tetrahydrofuran T=-40 - 20°C; 3: 2,5-dibromo-3-methylthiophene With Ni(dppp)Cl2 in tetrahydrofuran T=20°C; 12 h;
参考文献
Sheina, Elena E.; Liu, Jinsong; Lovu, Mihaela Corina; Laird, Darin W.; McCullough, Richard D.
Macromolecules, 2004 , vol. 37, # 10 p. 3526 - 3528
反应条件
hydrogen; aluminum oxide; molybdenum(VI) oxide in benzene T=400°C; 3 h; conversion; var. pretreatments; var. MoO3/Al2O3 ratio and quality of catalyst; Mechanism;
参考文献
Bernini, Maria C.; Gandara, Felipe; Iglesias, Marta; Snejko, Natalia; Gutierrez-Puebla, Enrique; Brusau, Elena V.; Narda, Griselda E.; Monge, M. Angeles
Chemistry - A European Journal, 2009 , vol. 15, # 19 p. 4896 - 4905
