188290-36-0合成路线 (共 917 条)
反应条件
phosphorus pentoxide
参考文献
Hartough; Kosak
Journal of the American Chemical Society, 1947 , vol. 69, p. 3098
反应条件
tin(IV) chloride in benzene
参考文献
Rao, S. Jagadishwar; Bhalerao, U. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1275 - 1276
反应条件
tin(IV) chloride in benzene
T=30°C; Friedel-Crafts acylation; 3 h;
参考文献
Matsubara, Hiroshi; Yasuda, Shinji; Ryu, Ilhyong
Synlett, 2003 , # 2 p. 247 - 249
反应条件
tin(IV) chloride in dichloromethane
T=23°C; Friedel-Crafts reaction; 4 h;
参考文献
Zhao, Weili; Carreira, Erick M.
Chemistry - A European Journal, 2007 , vol. 13, # 9 p. 2671 - 2688
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) -78 deg C, 1 h, 2.) r.t., overnight;
参考文献
Padwa, Albert; Hertzog, Donald L.; Nadler, William R.
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7072 - 7084
反应条件
tin(IV) chloride; Petroleum ether
参考文献
Bruson; Kroeger
Journal of the American Chemical Society, 1940 , vol. 62, p. 36,43
反应条件
aluminium trichloride; bromine
1.) CH2Cl2, -40 deg C, 2 h; rt, 2 days; 2.) glacial acetic acid, rt, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Belen'kii, L. I.; Yakubov, A. P.
Tetrahedron, 1984 , vol. 40, # 13 p. 2471 - 2477
反应条件
diethyl ether; phenyllithium
Behandeln des Reaktionsgemisches mit (+-)-3-Diaethylamino-buttersaeure-aethylester in Aether bei -20grad;
参考文献
Adamson
Journal of the Chemical Society, 1950 , p. 885,889
反应条件
tellurium; n-butyllithium; trifluoroacetic acid
1.) THF, cold, 10 min; RT, 60 min, 2.) 30 min, 2.) -78 deg C;
参考文献
Akiba, Mitsuo; Cava, Michael P.
Synthetic Communications, 1984 , vol. 14, # 12 p. 1119 - 1128
反应条件
acetic acid
T=70°C; 12 h;
参考文献
Stuhr-Hansen, Nicolai; Solling, Theis Ivan; Henriksen, Lars
Tetrahedron, 2011 , vol. 67, # 14 p. 2633 - 2643