188290-36-0合成路线 （共 917 条）
反应条件
aluminium trichloride; PhSeOCl in chloroform
T=40°C; 6 h;
参考文献
Kamigata, Nobumasa; Suzuki, Takashi; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 29 - 35
反应条件
aluminium trichloride in chloroform
T=40°C; 6 h;
参考文献
Kamigata, Nobumasa; Suzuki, Takashi; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 29 - 35
反应条件
aluminum tri-bromide; PhSeOCl in dichloromethane
3.5 h; Ambient temperature;
参考文献
Kamigata, Nobumasa; Suzuki, Takashi; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 29 - 35
反应条件
(NH4)2S2O8
1.) MeOH, 1 h, reflux 2.) MeOH, 1 h then reflux 1 h; Yield given. Multistep reaction;
参考文献
Engman, Lars; Eriksson, Per
Heterocycles, 1996 , vol. 43, # 4 p. 861 - 871
反应条件
aluminium trichloride in dichloromethane
T=40°C; 6 h; also with benzeneseleninyl bromide, various thiophenes, other conditions; Product distributionMechanism;
参考文献
Kamigata, Nobumasa; Suzuki, Takashi; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 29 - 35
反应条件
sodium acetate
T=250°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Leroy,J.; Rubinstein,M.
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 291
反应条件
n-butyllithium
1) ether, 2) ether, a) - 40 deg C, b) RT, overnight; Yield given. Multistep reaction;
参考文献
Hatanaka, Yasuo; Fukushima, Satoshi; Hiyama, Tamejiro
Tetrahedron, 1992 , vol. 48, # 11 p. 2113 - 2126
反应条件
calcium
1.5 h; Ambient temperature;
参考文献
Mochida, Kunio; Kojima, Kenji; Yoshida, Yasuhiro
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2255 - 2256
反应条件
aluminium trichloride in carbon disulfide
3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
反应条件
iron(III) chloride in carbon disulfide
3 h; Ambient temperature; Further byproducts given;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
