188290-36-0合成路线 （共 917 条）
反应条件
n-butyllithium 1.) THF, -20 deg C, 1 h, 2.) THF, -20 deg C, 1 h; Multistep reaction;
参考文献
Barbarella, Giovanna; Pudova, Olga; Arbizzani, Catia; Mastragostino, Marina; Bongini, Alessandro
Journal of Organic Chemistry, 1998 , vol. 63, # 5 p. 1742 - 1745
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane N2-atmosphere; stirring and refluxing thiophene with BuLi and TMEDA for 2 h, add. of excess Me2GeCl2, stirring at room temp. for 3 h; collection (filtration), washing (water, MeOH, hexane), drying (vac.); elem. anal.;
参考文献
Barrau; Rima; Akkari; Satge
Inorganica Chimica Acta, 1997 , vol. 260, # 1 p. 11 - 15
反应条件
mercury dibromide in benzene 12 h; Heating;
参考文献
Fujiwara, Shin-Ichi; Ogawa, Akiya; Kambe, Nobuaki; Ryu, Ilhyong; Sonoda, Noboru
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6121 - 6124
反应条件
aluminium trichloride in dichloromethane T=0°C; 2 h;
参考文献
Mourad; Wise; Townsend
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1583 - 1592
反应条件
aluminium trichloride in dichloromethane 4 h; Ambient temperature;
参考文献
Ohta, Akira; Kobayashi, Tomoshige; Kato, Hiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 8 p. 905 - 912
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.833333 h; 2: n-bromopentane in tetrahydrofuran; hexane T=-78 - 20°C; Further stages.;
参考文献
Zheng, Chunhong; Pu, Shouzhi; Xu, Jingkun; Luo, Mingbiao; Huang, Dechao; Shen, Liang
Tetrahedron, 2007 , vol. 63, # 25 p. 5437 - 5449
反应条件
Irradiation; Further byproducts given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 11 p. 1222 - 1226
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 11 p. 1469 - 1473
参考文献
Ertas, Erdal; Ozturk, Turan
Tetrahedron Letters, 2004 , vol. 45, # 17 p. 3405 - 3407
反应条件
bromine in chloroform 4 h; Heating;
参考文献
Nielsen, Christian B.; Bjornholm, Thomas
Organic Letters, 2004 , vol. 6, # 19 p. 3381 - 3384
参考文献
Meyer,V.; Kreis
Chemische Berichte, 1883 , vol. 16, p. 2172
Full Text Show Details
Volhard; Erdmann
Chemische Berichte, 1885 , vol. 18, p. 454
