188290-36-0合成路线 （共 917 条）
反应条件
1.) glow discharge, 2.) -196 deg C -> -80 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Skramstad, Jan; Chaudhry, Mohammed Shoaib; Garvang, Arne
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 509 - 512
反应条件
in dichloromethane
T=-78°C; Friedel-Crafts alkylation;
参考文献
Suga, Seiji; Nagaki, Aiichiro; Yoshida, Jun-Icih
Chemical Communications, 2003 , # 3 p. 354 - 355
反应条件
in dichloromethane
T=-78°C; Friedel-Crafts alkylation;
参考文献
Suga, Seiji; Nagaki, Aiichiro; Yoshida, Jun-Icih
Chemical Communications, 2003 , # 3 p. 354 - 355
反应条件
aluminium trichloride in dichloromethane
0.166667 h; Ambient temperature;
参考文献
Chambers, Jeffrey D.; Crawford, Jason; Williams, Haydn W. R.; Dufresne, Claude; Scheigetz, John; et al.
Canadian Journal of Chemistry, 1992 , vol. 70, # 6 p. 1717 - 1732
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2-
参考文献
Westfahl; Gresham
Journal of the American Chemical Society, 1954 , vol. 76, p. 1076,1077
反应条件
1: thiophene With n-butyllithium in diethyl ether; hexane
T=-40°C; 1 h; Inert atmosphere;
2: With sulfur in diethyl ether; hexane
T=-78 - 0°C; Inert atmosphere;
3: ethylene dibromide in diethyl ether; hexane
T=0 - 20°C; 18 h; Inert atmosphere;
参考文献
Wiles, Jason A.; Phadke, Avinash S.; Bradbury, Barton J.; Pucci, Michael J.; Thanassi, Jane A.; Deshpande, Milind
Journal of Medicinal Chemistry, 2011 , vol. 54, # 9 p. 3418 - 3425
反应条件
isopentyl nitrite
T=70 - 80°C;
参考文献
Vernin,G.; Metzger,J.
Journal of Organic Chemistry, 1975 , vol. 40, p. 3183 - 3189
反应条件
tert.-butylnitrite
2 h; Irradiation;
参考文献
Julliard,M. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 2941 - 2948
参考文献
Vernin,G. et al.
Helvetica Chimica Acta, 1976 , vol. 59, p. 1705 - 1724
反应条件
isopentyl nitrite
T=70 - 80°C;
参考文献
Vernin,G.; Metzger,J.
Journal of Organic Chemistry, 1975 , vol. 40, p. 3183 - 3189
