188290-36-0合成路线 (共 917 条)
参考文献
Volhard
Justus Liebigs Annalen der Chemie, 1892 , vol. 267, p. 180
反应条件
sodium acetate
extn. with hot ethanol;
参考文献
Obafemi, Craig A.
Journal of Organometallic Chemistry, 1981 , vol. 219, # 1 p. 1 - 7
反应条件
formaldehyd; ammonium chloride; acetic acid
anschliessendes Behandeln mit Methanol;
参考文献
Hartough; Meisel
Journal of the American Chemical Society, 1948 , vol. 70, p. 4018
反应条件
anschliessenden Behandeln mit Methanol;
参考文献
Hartough; Meisel
Journal of the American Chemical Society, 1948 , vol. 70, p. 4018
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Hartough et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1146,4013
反应条件
1: thiophene With potassium permanganate; acetic acid
Microwave irradiation;
2: pyrimidin-5-yl boronic acid 0.5 h; Microwave irradiation;
参考文献
Demir, Ayhan S.; Findik, Hamide; Saygili, Nezire; Tuna Subasi
Tetrahedron, 2010 , vol. 66, # 6 p. 1308 - 1312
反应条件
in acetonitrile
Irradiation;
参考文献
Allen,D.W. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 621 - 624
反应条件
in acetonitrile
Irradiation;
参考文献
Allen,D.W. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 621 - 624
反应条件
tin(IV) chloride in dichloromethane
T=20°C; Friedel-Crafts;
参考文献
Raposo, M. Manuela M.; Kirsch
Heterocycles, 2001 , vol. 55, # 8 p. 1487 - 1498
参考文献
Demerseman et al.
Journal of the Chemical Society, 1954 , p. 4193,4196
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran
T=-75°C; 1 h; Inert atmosphere;
2: With zinc(II) chloride−TMEDA in tetrahydrofuran
T=-75 - 20°C;
3: 1-bromo-4-nitro-benzene Further stages;
参考文献
Seggio, Anne; Priem, Ghislaine; Chevallier, Floris; Mongin, Florence
Synthesis, 2009 , # 21 p. 3617 - 3632