188290-36-0合成路线 （共 917 条）
反应条件
tert.-butylnitrite; ascorbic acid powder in dimethyl sulfoxide; acetonitrile
T=20°C; 12 h; Inert atmosphereGreen chemistry;
参考文献
Crisostomo, Fernando Pinacho; Martin, Tomas; Carrillo, Romen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 8 p. 2181 - 2185
Angew. Chem., 2014 , vol. 53, # 8 p. 2213 - 2217,5
反应条件
C33H25BF2I2N2 in dimethyl sulfoxide
T=20°C; 1 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalyst;
参考文献
Huang, Ling; Zhao, Jianzhang
RSC Advances, 2013 , vol. 3, # 45 p. 23377 - 23388
参考文献
Hardie; Thomson
Journal of the Chemical Society, 1957 , p. 2512,2517
反应条件
hydrogen bromide in acetic acid
1.) room temperature, 30 min, 2.) 50 deg C, 15 min;
参考文献
Scheytza, Holger; Reissig, Hans-Ulrich; Rademacher, Otto
Tetrahedron, 1999 , vol. 55, # 15 p. 4709 - 4720
反应条件
hydrogen bromide; acetic acid
T=5 - 20°C;
参考文献
Jorgensen, Mikkel; Krebs, Frederik C.
Journal of Organic Chemistry, 2005 , vol. 70, # 15 p. 6004 - 6017
反应条件
nitric acid
Beim Durchleiten eines mit Thiophendampf beladenen Luftstromes;
参考文献
Meyer,V.; Stadler
Chemische Berichte, 1884 , vol. 17, p. 2649
反应条件
beim Durchleiten von Luft;
参考文献
Meyer,V.; Stadler
Chemische Berichte, 1884 , vol. 17, p. 2649
Full Text Show Details
Babasinian
Journal of the American Chemical Society, 1928 , vol. 50, p. 2753
Full Text Show Details
Meyer,V.; Stadler
Chemische Berichte, 1885 , vol. 18, p. 531
参考文献
Levitt; Howard
Journal of the American Chemical Society, 1954 , vol. 76, p. 1951
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexanes
Inert atmosphere;
2: 6-methyl-2-oxo-1,2-dihydropyrimidine-5-carboxylic acid ethyl ester in tetrahydrofuran; hexanes
T=-40°C; Inert atmosphere;
参考文献
Singh, Kamaljit; Arora, Divya; Falkowski, Danielle; Liu, Qingxin; Moreland, Robert S.
European Journal of Organic Chemistry, 2009 , # 19 p. 3258 - 3264
反应条件
ethanol; boron trifluoride diethyl etherate in nitromethane
T=20°C; 12 h; 3-oxobutylation also of substituted thiophenes, temperature also 100 deg C, reaction time varied; Product distribution;
参考文献
Dujardin, Gilles; Poirier, Jean-Marie
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 900 - 909
