188290-36-0合成路线 （共 917 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane
addn. and stirring BuLi in hexane and thiophene in dry THF at -30°C under N2 (1 h), addn. of HgCl2 at -55°C, stirring at -55°C (1 h), warming to room temp., pptn.; filtration at the pump, washing with THF-light petroleum (1:1) and H2O, drying in vac.;
参考文献
Pinhey, John T.; Roche, Eric G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2415 - 2422
反应条件
ruthenium trichloride
140 h;
参考文献
Jaouhari, Rabih; Guenot, Pierre; Dixneuf, Pierre H.
Journal of the Chemical Society, Chemical Communications, 1986 , # 16 p. 1255 - 1257
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene
24 h; Heating;
参考文献
Wenkert, Ernest; Leftin, Michael H.; Michelotti, Enrique L.
Journal of the Chemical Society, Chemical Communications, 1984 , # 9 p. 617 - 618
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in benzene
24 h; Heating;
参考文献
Wenkert, Ernest; Leftin, Michael H.; Michelotti, Enrique L.
Journal of the Chemical Society, Chemical Communications, 1984 , # 9 p. 617 - 618
反应条件
1: thiophene With n-butyllithium in diethyl ether
T=20°C; 2 h;
2: chloro-diphenylphosphine in diethyl ether
T=20°C; Further stages.;
参考文献
Stott, Tracey L.; Wolf, Michael O.
Journal of Physical Chemistry B, 2004 , vol. 108, # 49 p. 18815 - 18819
反应条件
palladium diacetate; caesium carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl-formamide
T=100°C; 2 h; Inert atmosphere;
参考文献
Liang, Yong; Gloudeman, Jennifer; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4094 - 4103
反应条件
(i) nBuLi, HMPT, Et2O, (ii) /BRN= 969135/, THF; Multistep reaction;
参考文献
Woo, H. G.; Han, S. Y.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, p. 803 - 804
反应条件
anhydrous magnesium perchlorate
6 h; Heating;
参考文献
Bandgar; Kamble; Bavikar
Journal of Chemical Research - Part S, 2003 , # 5 p. 287 - 289
反应条件
tetrakis(triphenylphosphine) palladium(0); N,N-dimethyl acetamide; potassium acetate
T=150°C; 12 h;
参考文献
Ohta, Akihiro; Akita, Yasuo; Ohkuwa, Teruya; Chiba, Mari; Fukunaga, Ryuichi; et al.
Heterocycles, 1990 , vol. 31, # 11 p. 1951 - 1958
参考文献
Smith; Boyer
Journal of the American Chemical Society, 1951 , vol. 73, p. 2626,2629
