188290-36-0合成路线 (共 917 条)
参考文献
Koldobskii; Vakhmistrov; Solodova; Shilova; Kalinin
Doklady Chemistry, 2002 , vol. 387, # 1-3 p. 289 - 292
反应条件
potassium acetate; 18-crown-6 ether
1.5 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
参考文献
Buu-Hoi; Hoan
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1455,1466
反应条件
hydrogenchloride; sodium hydroxide; sodium nitrite
参考文献
Buu-Hoi; Hoan
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1455,1466
反应条件
tert.-butylhydroperoxide; [VIVO(N,N-bis(o-hydroxybenzaldehyde)phenylene diamine)]
T=40°C; 6 h;
参考文献
Ogunlaja, Adeniyi S.; Khene, Samson; Antunes, Edith; Nyokong, Tebello; Torto, Nelson; Tshentu, Zenixole R.
Applied Catalysis A: General, 2013 , vol. 462-463, p. 157 - 167
反应条件
trifluoromethylsulfonic anhydride; bis(N-methylpyridinium) sulfate
0.0833333 h;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Chemistry Letters, 2010 , vol. 39, # 4 p. 390 - 391
反应条件
N(Et)4ClO4; trichloroacetic acid in dichloromethane
2 h; Ambient temperatureworking pot.: 2.2 V vs SCE;
参考文献
Do, Quang Tho; Elothmani, Driss; Simonet, Jacques; Guillanton, Georges Le
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 789 - 793
反应条件
1: 3-chloropropanoyl chloride With AlCl3, aluminium chloride in dichloromethane
T=-5°C; Friedel Crafts Acylation; 0.166667 h;
2: thiophene in dichloromethane
T=-5°C; Friedel Crafts Acylation; 1 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2004/43931 A1, 2004 ;
Location in patent: Page 30-31 ;
WO 2004/043931 A1
反应条件
aluminium trichloride in carbon disulfide
3 h; Ambient temperature;
参考文献
El-Khagawa, Ahmed M.; El-Zohry, Maher F.; Ismail, Mohamed T.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 33, p. 25 - 32
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5099,5101