188290-36-0合成路线 （共 917 条）
反应条件
(i) nBuLi, Et2O, (ii) /BRN= 107326/, (iii) KMnO4; Multistep reaction;
参考文献
Gronowitz,S.; Roee,J.
Acta Chemica Scandinavica (1947-1973), 1965 , vol. 19, p. 1741 - 1748
反应条件
phosphoric acid
T=120°C;
参考文献
Pines et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5173
参考文献
Pines et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5173
反应条件
1: With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether; hexane
T=0 - 20°C; 2 h; Inert atmosphere;
2: With magnesium bromide in tetrahydrofuran; diethyl ether; hexane
T=0°C; 0.5 h; Inert atmosphere;
参考文献
Dhakal, Ramesh C.; Dieter, R. Karl
Organic Letters, 2014 , vol. 16, # 5 p. 1362 - 1365
反应条件
C19H10F12S in 1,2-dichloro-ethane
T=83°C; 2 h; Inert atmosphereMolecular sieve;
参考文献
Watanabe, Naruhisa; Matsugi, Aoi; Nakano, Keiji; Ichikawa, Yoshiyasu; Kotsuki, Hiyoshizo
Synlett, 2014 , vol. 25, # 3 art. no. ST-2013-U0808-L, p. 438 - 442
反应条件
palladium dichloride in 1,2-dichloro-ethane
T=80°C; Tsuji-Trost reaction; 20 h; Sealed tube;
参考文献
Yuan, Feng-Quan; Gao, Lian-Xun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 18 p. 5289 - 5291
参考文献
Levi
Chemische Berichte, 1886 , vol. 19, p. 1624
反应条件
carbon disulfide; tin(IV) chloride
参考文献
Stadnikow; Goldfarb
Chemische Berichte, 1928 , vol. 61, p. 2342
Full Text Show Details
Goldfarb
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1930 , vol. 62, p. 1073,1081
Chem. Zentralbl., 1930 , vol. 101, # II p. 3558
参考文献
Stadnikow; Goldfarb
Chemische Berichte, 1928 , vol. 61, p. 2342
Full Text Show Details
Goldfarb
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1930 , vol. 62, p. 1073,1081
Chem. Zentralbl., 1930 , vol. 101, # II p. 3558
反应条件
n-butyllithium
1.) THF, hexane, -30 deg C, 1 h, 2.) THF, hexane, -70 deg C, 0.5 h, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Kumamoto, Takanobu; Hosoya, Kumiko; Kanzaki, Satoshi; Masuko, Kazuhiro; Watanabe, Mikio; Shirai, Kozo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 10 p. 3097 - 3102
