反式-2-羟基环己烷甲酸乙酯合成路线 (共 14 条)
反应条件
Candida antarctica lipase B in various solvent(s) T=30°C; 2.66667 h;
参考文献
Levy, Laura M.; Lavandera, Ivan; Gotor, Vicente
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 18 p. 2572 - 2577
反应条件
Candida antarctica lipase B; water in tert-butyl methyl ether T=30°C; 0.5 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Forro, Eniko; Galla, Zsolt; Fueloep, Ferenc
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 98, p. 92 - 97
反应条件
1: vinyl acetate; ethyl cis-(±)-2-hydroxycyclopentane-1-carboxylate With Candida antarctica lipase B; water in tert-butyl methyl ether T=30°C; 0.5 h; Resolution of racemateEnzymatic reaction; 2: diazomethane enantioselective reaction;
参考文献
Forro, Eniko; Galla, Zsolt; Fueloep, Ferenc
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 98, p. 92 - 97
反应条件
1: P2O5
2: NaOEt
View Scheme
参考文献
Scharf,H.-D.; Korte,F.
Chemische Berichte, 1964 , vol. 97, p. 2425 - 2433