2-苯基-5-三氟甲基吡啶合成路线 （共 5 条）
反应条件
1: With palladium diacetate; xantphos in N-dodecane; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; 0.0833333 h; Inert atmosphereGlovebox; 2: With cesium hydroxide monohydrate in N-dodecane; water; butan-1-ol T=25°C; Suzuki-Miyaura Coupling; Inert atmosphereGlovebox;
参考文献
Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259,12
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Yang, Junfeng; Liu, Sijia; Zheng, Jian-Feng; Zhou, Jianrong
European Journal of Organic Chemistry, 2012 , # 31 p. 6248 - 6259
反应条件
C60H48Cl2FeP4; Zn(C6H4-4-OMe)2 in tetrahydrofuran; toluene T=115°C; Suzuki coupling; 16 h; Inert atmosphere;
参考文献
Bedford, Robin B.; Hall, Mark A.; Hodges, George R.; Huwe, Michael; Wilkinson, Mark C.
Chemical Communications, 2009 , # 42 p. 6430 - 6432
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=130°C; Inert atmosphereSealed tube;
参考文献
Petiot, Pauline; Gagnon, Alexandre
European Journal of Organic Chemistry, 2013 , # 24 p. 5282 - 5289
反应条件
P(NC5H10)3; nickel dichloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 1 h;
参考文献
Gerber, Roman; Frech, Christian M.
Chemistry - A European Journal, 2011 , vol. 17, # 42 p. 11893 - 11904
反应条件
lithium aluminium tetrahydride; niobium pentachloride in 1,4-dioxane
4 h; Heating;
参考文献
Fuchibe, Kohei; Ohshima, Yoshitaka; Mitomi, Ken; Akiyama, Takahiko
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1158 - 1167
