反应条件
1: 65 percent / 18-crown-6-ether / dimethylsulfoxide / 12 h / 85 °C 2: 96 percent / DIBAL / toluene / 1 h / -10 °C 3: 78 percent / LiAlH4 / diethyl ether / 3 h / Ambient temperature 4: 100 percent / (TMS)2SO4 / 1,2-dichloro-ethane; methanol / 0.03 h / Ambient temperature 5: TsCl, pyridine View Scheme
参考文献
Tanimoto, Hisahide; Oritani, Takayuki
Tetrahedron Asymmetry, 1996 , vol. 7, # 6 p. 1695 - 1704
