(4R)-3-[(2E)-2-戊烯酰]-4-苯基-1,3-恶唑烷-2-酮合成路线 （共 6 条）
反应条件
n-butyllithium in tetrahydrofuran T=-78°C;
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628
反应条件
1: CuBr, DMS / tetrahydrofuran / 1 h / 0 °C 2: 1.) H3O+, 2.) Na2CO3 / 2.) H2O, CH2Cl2 View Scheme
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628
反应条件
1: CuBr, DMS / tetrahydrofuran / 1 h / 0 °C 2: 1.) H3O+, 2.) Na2CO3 / 2.) H2O, CH2Cl2 5: 67 percent / t-BuOK / tetrahydrofuran / 0 °C 6: H2 / Pd/C / methanol; ethyl acetate 7: 81 percent / pyridine / CH2Cl2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 15 p. 3627 - 3628
反应条件
1: CuBr, DMS / tetrahydrofuran / 1 h / 0 °C 2: 1.) H3O+, 2.) Na2CO3 / 2.) H2O, CH2Cl2 View Scheme
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628
反应条件
1: CuBr, DMS / tetrahydrofuran / 1 h / 0 °C 2: 1.) H3O+, 2.) Na2CO3 / 2.) H2O, CH2Cl2 5: 67 percent / t-BuOK / tetrahydrofuran / 0 °C View Scheme
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628
反应条件
1: CuBr, DMS / tetrahydrofuran / 1 h / 0 °C 2: 1.) H3O+, 2.) Na2CO3 / 2.) H2O, CH2Cl2 View Scheme
参考文献
Judge; Phillips; Morris; Lovasz; Romines; Luke; Tulinsky; Tustin; Chrusciel; Dolak; Mizsak; Watt; Vander Velde; Strohbach; Gammill
Journal of the American Chemical Society, 1997 , vol. 119, # 15 p. 3627 - 3628
