反应条件
1: K2OsO4*2H2O, K3Fe(CN)6, DHQD-PHN / H2O; 2-methyl-propan-2-ol
2: H2SO4 / tetrahydrofuran / 0 °C
3: 80 percent / NaH / dimethylformamide
4: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating
5: 28 percent / pyridine*HF / dioxane
6: 86 percent / 50percent TFA / CH2Cl2
View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
