反应条件
1: 1.) EtMgBr, 2.) CuI / 1.) THF, 40 deg C, 30 min, 2.) THF, a) 50 deg C, 3 h, b) RT, overnight
2: H2, quinoline / Pd/BaSO4 / ethyl acetate
3: lithium t-butyl thiolate / dimethylformamide
View Scheme
参考文献
Tyman, John H.P.; Visani
Chemistry and Physics of Lipids, 1997 , vol. 85, # 2 p. 157 - 174
