N,N-二乙基-3-苯基丙酰胺合成路线 （共 30 条）
反应条件
4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium chloride in methanol
T=20°C; 2 h;
参考文献
Kunishima, Munetaka; Kawachi, Chiho; Hioki, Kazuhito; Terao, Keiji; Tani, Shohei
Tetrahedron, 2001 , vol. 57, # 8 p. 1551 - 1558
反应条件
palladium 10 on activated carbon; hydrogen in tetrahydrofuran
T=25°C; P=750.075 Torr;
参考文献
Stefane, Bogdan; Polanc, Slovenko
Tetrahedron, 2009 , vol. 65, # 11 p. 2339 - 2343
参考文献
Maxim
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 182, p. 1395
Annales de Chimie (Cachan, France), 1928 , vol. <10> 9, p. 69,76
反应条件
1: (E)-cinnamaldehyde With trimethylsilyl cyanide; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=25°C; 4.5 h;
2: diethylamine in acetonitrile
参考文献
Kawabata, Hirotoshi; Hayashi, Masahiko
Tetrahedron Letters, 2002 , vol. 43, # 32 p. 5645 - 5647
反应条件
C29H55IrN3P2(1+)*Cl(1-); potassium tert-butylate in toluene
T=120°C; 15 h; Schlenk techniqueInert atmosphereGlovebox;
参考文献
Guo, Le; Liu, Yinghua; Yao, Wubing; Leng, Xuebing; Huang, Zheng
Organic Letters, 2013 , vol. 15, # 5 p. 1144 - 1147
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Concellon, Jose M.; Huerta, Monica; Bardales, Eva
Tetrahedron, 2004 , vol. 60, # 44 p. 10059 - 10065
反应条件
1: With N-chloro-succinimide in dichloromethane
Inert atmosphereCooling with ice;
2: With (5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; benzotriazol-1-ol; triethylamine in dichloromethane
T=20°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Kuwano, Satoru; Harada, Shingo; Oriez, Raphael; Yamada, Ken-Ichi
Chemical Communications, 2012 , vol. 48, # 1 p. 145 - 147
反应条件
2-pentafluorophenyl-6,17dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; water; triethylamine in dichloromethane
T=20°C; 0.166667 h; Inert atmosphere; chemoselective reaction;
参考文献
Kuwano, Satoru; Harada, Shingo; Oriez, Raphael; Yamada, Ken-Ichi
Chemical Communications, 2012 , vol. 48, # 1 p. 145 - 147
反应条件
4-(N,N-dimethlyamino)pyridine in chloroform
T=70°C; 4 h; Inert atmosphere;
参考文献
Bai, Jianfei; Zambron, Bartosz K.; Vogel, Pierre
Organic Letters, 2014 , vol. 16, # 2 p. 604 - 607
反应条件
methanol; samarium diiodide in tetrahydrofuran
T=25°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Concellon, Jose M.; Bardales, Eva
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9492 - 9495
