N,N-二乙基-3-苯基丙酰胺合成路线 （共 30 条）
反应条件
in dichloromethane
12 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
in dichloromethane
12 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
1: 1,3-dicyclohexylcarbodiimide / CH2Cl2 / from 0 deg C to RT
2: 90 percent / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
in dichloromethane
60 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h / -78 °C
1.2: tetrahydrofuran / 1 h / -78 °C
2.1: sodium hydride / CH2Cl2 / 2.5 h / 25 °C
3.1: SmI2; MeOH / tetrahydrofuran / 0.5 h / 25 °C
View Scheme
参考文献
Concellon, Jose M.; Bardales, Eva
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9492 - 9495
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / 0.17 h / -78 °C
1.2: tetrahydrofuran / 1 h / -78 °C
2.1: sodium hydride / CH2Cl2 / 2.5 h / 25 °C
3.1: SmI2; MeOH / tetrahydrofuran / 0.5 h / 25 °C
View Scheme
参考文献
Concellon, Jose M.; Bardales, Eva
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9492 - 9495
反应条件
1: EDC
2: 69 percent / SmI2, LiCl / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Hughes, Adam D.; Price, David A.; Simpkins, Nigel S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1295 - 1304
反应条件
in dichloromethane
0.5 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Ferreira, J. Albert
Tetrahedron, 1996 , vol. 52, # 28 p. 9347 - 9366
反应条件
trichlorophosphate in chloroform
参考文献
Deshmukh, Sanjay Y.; Kelkar, Shriniwas L.; Wadia, Murzban S.
Synthetic Communications, 1990 , vol. 20, # 6 p. 855 - 863
