1-(4-氯苯氧基)-2-丙酮合成路线 （共 6 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
MERCK and CO., INC.
Patent: WO2009/5672 A1, 2009 ;
Location in patent: Page/Page column 70 ;
反应条件
oxygen; lithium chloride; copper dichloride; {Pd2(MeCN)2(PHT)[(S)-Tol-BINAP]}(BF4)2 in tetrahydrofuran; water T=25°C; P=760 Torr; Title compound not separated from byproducts;
参考文献
El-Qisairi, Arab K; Qaseer, Hanan A; Henry, Patrick M
Journal of Organometallic Chemistry, 2002 , vol. 656, # 1-2 p. 168 - 176
反应条件
dirhodium tetraacetate in dichloromethane T=20°C; 12 h; Kinetics; Further Variations:Reagents;
参考文献
Qu, Zhaohui; Shi, Weifeng; Wang, Jianbo
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 217 - 219
反应条件
1: 83 percent / K2CO3 / acetone / 2 h / Heating 2: O2; LiCl; CuCl2 / {Pd2(MeCN)2(PHT)[(S)-Tol-BINAP]}(BF4)2 / tetrahydrofuran; H2O / 25 °C / 760 Torr View Scheme
参考文献
El-Qisairi, Arab K; Qaseer, Hanan A; Henry, Patrick M
Journal of Organometallic Chemistry, 2002 , vol. 656, # 1-2 p. 168 - 176
反应条件
sodium hydroxide; acetone
参考文献
Bokarew; Mel'nikow
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 2014,2022; engl. Ausg. S. 1979, 1986
反应条件
in acetone 3 h; Heating / reflux;
参考文献
SYNGENTA PARTICIPATIONS AG
Patent: WO2004/797 A1, 2003 ;
Location in patent: Page 28 ;
