2-methylpropane-2-thiol in methanol T=25°C; Decomposition; reduction; Photolysis; Title compound not separated from byproducts;

2-methylpropane-2-thiol in methanol T=25°C; Decomposition; reduction; Photolysis; Title compound not separated from byproducts;

in benzene T=7°C; Decomposition; Photolysis; Title compound not separated from byproducts;

<b>Multi-step reaction with 3 steps<br /> </b>1.1: 90 percent / potassium cyanide; 18-crown-6 / dimethylformamide / 0.67 h / 0 &deg;C<br />2.1: CuI / diethyl ether; hexane / 3.5 h / -78 &deg;C<br />2.2: 20 percent / acetic acid; water / diethyl ether; hexane<br />3.1: 91 percent / 4-(dimethylamino)pyridine; pyridine / CH₂Cl₂ / 0.33 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 77 percent / HF*pyridine / tetrahydrofuran; pyridine / 5 h / 20 &deg;C<br />2: 91 percent / 4-(dimethylamino)pyridine; pyridine / CH₂Cl₂ / 0.33 h<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '103233', constants.ctx, '0')">pyridine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '110354', constants.ctx, '0')">4-(N,N-dimethlyamino)pyridine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />Acetylation;&nbsp;0.333333&nbsp;h;&nbsp;<br /> &nbsp;