4-(N,N-二甲基氨基亚甲基)-2-甲基-5-噁唑啉酮合成路线 （共 6 条）
反应条件
trichlorophosphate T=40 - 45°C; 1 h;
参考文献
Kralj, Lucija; Hvala, Ales; Svete, Jurij; Golic, Ljubo; Stanovnik, Branko
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 1 p. 247 - 255
反应条件
1: With N,N-dimethyl-formamide; trichlorophosphate T=0 - 45°C; 1.5 h; 2: With ammonia in water T=0 - 10°C; 1 h;
参考文献
Ruck, Rebecca T.; Huffman, Mark A.; Stewart, Gavin W.; Cleator, Ed; Kandur, Wynne V.; Kim, Mary M.; Zhao, Dalian
Organic Process Research and Development, 2012 , vol. 16, # 8 p. 1329 - 1337
参考文献
Takahashi, Daisuke; Izawa, Kunisuke; Kashiwagi, Tatsumi; Onoye, Hiromi; Williams, Robert M.
Heterocycles, 2012 , vol. 85, # 9 p. 2213 - 2229,17
反应条件
methanol; sodium hydroxide
参考文献
Ruck, Rebecca T.; Huffman, Mark A.; Stewart, Gavin W.; Cleator, Ed; Kandur, Wynne V.; Kim, Mary M.; Zhao, Dalian
Organic Process Research and Development, 2012 , vol. 16, # 8 p. 1329 - 1337
反应条件
1: 78 percent / K2CO3 / 0.5 h / Heating
2: 24 percent / AcOH / 1 h / Heating
View Scheme
参考文献
Kralj, Lucija; Hvala, Ales; Svete, Jurij; Golic, Ljubo; Stanovnik, Branko
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 1 p. 247 - 255
反应条件
methanol; sodium hydroxide
参考文献
Ruck, Rebecca T.; Huffman, Mark A.; Stewart, Gavin W.; Cleator, Ed; Kandur, Wynne V.; Kim, Mary M.; Zhao, Dalian
Organic Process Research and Development, 2012 , vol. 16, # 8 p. 1329 - 1337
