1: oxalyl dichloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Cooling with ice 2: ammonia; triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere 3: ethanol / 12 h / Reflux 4: water; sodium hydroxide / 1 h / Reflux View Scheme
参考文献
Thuo, Martin M.; Reus, William F.; Simeone, Felice C.; Kim, Choongik; Schulz, Michael D.; Yoon, Hyo Jae; Whitesides, George M.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10876 - 10884
1: ethanol / 12 h / Reflux 2: water; sodium hydroxide / 1 h / Reflux View Scheme
参考文献
Thuo, Martin M.; Reus, William F.; Simeone, Felice C.; Kim, Choongik; Schulz, Michael D.; Yoon, Hyo Jae; Whitesides, George M.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10876 - 10884
1: ammonia; triethylamine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere 2: ethanol / 12 h / Reflux 3: water; sodium hydroxide / 1 h / Reflux View Scheme
参考文献
Thuo, Martin M.; Reus, William F.; Simeone, Felice C.; Kim, Choongik; Schulz, Michael D.; Yoon, Hyo Jae; Whitesides, George M.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10876 - 10884
