4,4'-二甲基-反-二苯乙烯合成路线 （共 112 条）
反应条件
1: (E)-trimethyllt;2-(4-methylphenyl)ethenylgt;silane With boron trichloride in dichloromethane T=0°C; Substitution; 2 h; 2: 4-toluenediazonium tetrafluoroborate With palladium diacetate in 1,4-dioxane T=20°C; Substitution; 24 h; Further stages.;
参考文献
Babudri, Francesco; Farinola, Gianluca M.; Naso, Francesco; Panessa, Daniela
Journal of Organic Chemistry, 2000 , vol. 65, # 5 p. 1554 - 1557
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Li, Zhifang; Zhang, Yongmin
Journal of Chemical Research - Part S, 2003 , # 6 p. 340 - 341
反应条件
tetrachlorosilane; zinc in dichloromethane T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 48, # 25 p. 4395 - 4398
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride in tetrahydrofuran T=65°C; Hiyama coupling; 1 h; Inert atmosphere; stereoselective reaction;
参考文献
Pawluc, Piotr; Hreczycho, Grzegorz; Suchecki, Andrzej; Kubicki, Maciej; Marciniec, Bogdan
Tetrahedron, 2009 , vol. 65, # 28 p. 5497 - 5502
反应条件
cadmium(II) sulphide in dichloromethane Irradiation;
参考文献
Hasegawa, Tadashi; Mayo, Paul de
Journal of the Chemical Society, Chemical Communications, 1985 , # 21 p. 1534 - 1535
反应条件
diethyl sodio phosphonate in benzene T=130°C; 11.5 h; sealed tube;
参考文献
Minami, Toru; Matsuzaki, Narihide; Ohshiro, Yoshiki; Agawa, Toshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1731 - 1738
反应条件
H5PV2Mo10O40(1,11); hydrogen; Pt(N-(2,6-diisopropylphenyl)pyrazin-2-ylmethanimine)Cl2 T=100°C; P=1900.13 Torr; 18 h; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 38 p. 3957 - 3959
反应条件
potassium tert-butylate in ethanol 1 h;
参考文献
Warner, Philip; Sutherland, Robert
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6294 - 6300
反应条件
sodium methylate in methanol T=50°C; Wittig reaction; 3.5 h; Inert atmosphere;
参考文献
Letters in Organic Chemistry, , vol. 9, # 6 p. 427 - 434
反应条件
potassium phosphate; [Rh(OH)(cycloocta-1,5-diene)]2; 1,4-di(diphenylphosphino)-butane in 1,4-dioxane T=100°C; 3 h; Schlenk techniqueInert atmosphere;
参考文献
Matsuda, Takanori; Suzuki, Kentaro; Miura, Norio
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3396 - 3400
