4,4'-二甲基-反-二苯乙烯合成路线 （共 112 条）
反应条件
1: 74 percent / diethylamine, triphenylphosphine, palladium chloride, cuprous iodide / 8 h / 54 - 55 °C 2: 93 percent / hydrogen / Pd-CaCO3 / ethanol / 40 - 50 °C 3: iodine / light petroleum / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 308 - 311
Zhurnal Organicheskoi Khimii, , vol. 18, # 2 p. 355 - 359
参考文献
Journal of the American Chemical Society, , vol. 52, p. 3633
反应条件
{((i-PrO)3P)2Rh}2(.mu.-H)2; hydrogen in deuterated toluene T=20°C; studies of the intermediate structure; Mechanism;
参考文献
Journal of the American Chemical Society, , vol. 105, # 11 p. 3546 - 3556
反应条件
sulfur dioxide in ethanol T=20°C; Yield given;
参考文献
Chemische Berichte, , vol. 114, # 2 p. 787 - 801
反应条件
Cu(II) perchlorate in acetonitrile T=20°C; 0.3 h; Yield given;
参考文献
Chemistry Letters, , p. 1895 - 1898
反应条件
indium(III) chloride; sodium tetrahydroborate in acetonitrile T=-15 - 20°C; 15 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 1-2 p. 247 - 250
反应条件
potassium hydroxide; 18-crown-6 ether in dichloromethane T=-78°C; Wittig reaction; 6 h;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 11 p. 1313 - 1319
反应条件
1: 1.) sodium borohydride / 1.) THF, water, 0 deg C, 2.) 25 deg C, overnight 2: 95 percent / acetonitrile / 0.5 h / -10 °C 3: 24 percent / NaNH2, NH3 (liquid) / 1 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 6 p. 954 - 959
反应条件
1: 95 percent / acetonitrile / 0.5 h / -10 °C 2: 24 percent / NaNH2, NH3 (liquid) / 1 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 6 p. 954 - 959
