4,4'-二甲基-反-二苯乙烯合成路线 (共 112 条)
反应条件
1: 63 percent / tetrahydrofuran / 1 h / Heating 2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, -78 deg C to rt, 3 h View Scheme
参考文献
Tetrahedron, , vol. 54, # 50 p. 15361 - 15370
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 549 - 553
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 12 h; Heating;
参考文献
Chan, T. H.; Li, J. S.; Aida, T.; Harpp, David N.
Tetrahedron Letters, 1982 , vol. 23, # 8 p. 837 - 840
反应条件
1: 75 percent / NaBH4 / dimethylsulfoxide / 12 h / 70 °C 2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min; 2.) THF, r.t., 12 h View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 36 p. 6733 - 6736
反应条件
9,10-anthracenedicarbonitrile in acetonitrile T=20°C; 5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 25, # 13 p. 1367 - 1370
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 48 h; Heating;
参考文献
Tetrahedron Letters, , vol. 23, # 8 p. 837 - 840
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 24 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 375 - 380
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 35 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 375 - 380
反应条件
potassium hydroxide in tetrahydrofuran Heating; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 54, # 50 p. 15361 - 15370
反应条件
sulfur T=200 - 210°C; im geschlossenen Rohr;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 21, p. 455