4,4'-二甲基-反-二苯乙烯合成路线 (共 112 条)
反应条件
[{(ZnI2)3(tris(4-pyridyl)triazine)2}*x(C6H5NO2)]n in cyclohexane 72 h; Irradiation; optical yield given as percent de;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 32 p. 5507 - 5509
反应条件
sodium ethanolate in N,N-dimethyl-formamide Wittig-Horner reaction;
参考文献
Science China Chemistry, , vol. 54, # 11 p. 1735 - 1744
反应条件
aluminium silicate T=400 - 600°C;
参考文献
Doklady Akademii Nauk SSSR, , vol. 106, p. 271
Doklady Chemistry, 106-111 <1956> 43
反应条件
T=600°C; P=0.001 - 0.1 Torr; 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ferguson, George; Lough, Alan J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 875 - 880
反应条件
1: acetonitrile / 12 h / Reflux 2: sodium hydride / benzene View Scheme
参考文献
Medicinal Chemistry Research, , vol. 20, # 8 p. 1158 - 1163
反应条件
zinc bei der Destillation;
参考文献
Chemische Berichte, , vol. 6, p. 1504
反应条件
tellurium; n-butyllithium 1) in THF, 0 deg C, 2) RT, 3h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3559 - 3563
反应条件
T=600°C; P=0.001 - 0.1 Torr; 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ferguson, George; Lough, Alan J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 875 - 880
反应条件
in tetrahydrofuran 1.) -30 deg C, 1 h, 2.) r.t., 18 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 1700 - 1702
反应条件
sodium methylate; triphenylphosphine 1.) xylene, reflux, 6 h, 2.) CH2Cl2, THF, reflux, overnight; Multistep reaction;
参考文献
Journal of Chemical Physics, , vol. 91, # 2 p. 943 - 952