反应条件
1.1: Et3N; 2,4,6-trichlorobenzoyl chloride / tetrahydrofuran / 0.33 h / 20 °C 1.2: 88 percent / DMAP / toluene; tetrahydrofuran / 1 h 2.1: 99 percent / HF*pyridine / tetrahydrofuran 3.1: 49 percent / 3,3-dimethyldioxirane / CH2Cl2 / -35 °C View Scheme
参考文献
Dongfang, Meng; Bertinato, Peter; Balog, Aaron; Su, Dai-Shi; Kamenecka, Ted; et al.
Journal of the American Chemical Society, 1997 , vol. 119, # 42 p. 10073 - 10092