三乙氧基[4-(三氟甲基)苯基]硅烷合成路线 （共 14 条）
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=20°C; sonochemical Barbier-type reaction; 0.5 h; Irradiationsonication;
参考文献
Tetrahedron Letters, , vol. 47, # 39 p. 7085 - 7087
反应条件
NH4I; potassium fluoride; Cu(NO3)2*3H2O; oxygen T=140°C; 25 h; Schlenk technique;
参考文献
Wang, Zhen; Chang, Sukbok
Organic Letters, 2013 , vol. 15, # 8 p. 1990 - 1993
反应条件
sodium hydroxide; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane T=80°C; 4 h;
参考文献
Synthesis, , # 15 p. 2231 - 2233
反应条件
CM-phos; tetrabutyl ammonium fluoride; palladium diacetate; acetic acid in tert-butyl alcohol T=90°C; Hiyama cross-coupling; 16 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 2 p. 317 - 320
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); BaO; silver(l) oxide in acetone T=23 - 90°C; 2 h; regioselective reaction;
参考文献
Tang, Pingping; Ritter, Tobias
Tetrahedron, 2011 , vol. 67, # 24 p. 4449 - 4454
反应条件
copper(l) iodide; cesium fluoride in N,N-dimethyl-formamide T=120°C; Hiyama Coupling; 12 h; Inert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Vangala, Adarsh S.; Giri, Ramesh
Organic Letters, 2013 , vol. 15, # 20 p. 5378 - 5381
反应条件
copper(l) iodide; cesium fluoride; N,N-dimethyl-2-(diphenylphosphino)benzeneaniline in N,N-dimethyl-formamide
T=120°C; Hiyama Coupling; 24 h; Inert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Vangala, Adarsh S.; Giri, Ramesh
Organic Letters, 2013 , vol. 15, # 20 p. 5378 - 5381
反应条件
sodium hydroxide; methyl-ethyl phosphite; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane
T=80°C; 8 h;
参考文献
Murata; Shimazaki; Watanabe; Masuda
Synthesis, 2001 , # 15 p. 2231 - 2233
反应条件
copper(l) iodide; cesium fluoride; N,N-dimethyl-2-(diphenylphosphino)benzeneaniline in N,N-dimethyl-formamide
T=120°C; Hiyama Coupling; 24 h; Inert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Vangala, Adarsh S.; Giri, Ramesh
Organic Letters, 2013 , vol. 15, # 20 p. 5378 - 5381
反应条件
sodium hydroxide; tetrabutylammomium bromide; 4,4'-dichlorobenzophenone oxime-derived palladacycle
T=120°C; Hiyama coupling; P=7500.6 Torr; 0.166667 h; microwave irradiation;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 7-8 p. 945 - 952
