反应条件
in further solvent(s) further solvent: hexachloropropene; refluxing under exclusion of moisture for 4 h, cooling, crystn.;; filtration, washing with cold CCl4, pumping off remaining chlorinated hydrocarbons;;
参考文献
Porterfield, W. W.; Tyree, S. Y.
Inorganic Syntheses, 1967 , vol. 9, p. 133 - 136
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Gmelin Handbook: Nb: MVol.B1, 83, page 177 - 180
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Pitt, B. M.; Wagner, E. L.; Miller, A. J.
N.S.A., AECD-3965 (1955) 1/6 1956 , vol. 10, p. 3546