反应条件
in tetrahydrofuran
N2 atmosphere, addn. of soln. of C3Cl6 to soln. of Ni compound at -15°C, (6 h) while removing of the reaction atmosphere by a stream of nitrogen, standing (room temp., 2 d); evapn. to dryness (vacuum), washing (water, methanol and THF), extn. (DMSO), addn. of aq. (N(C2H5)4)Cl with stirring, filtration, washing (methanol), extn. (CH3CN), filtration, pptn. (diisopropyl ether); elem. anal.;
参考文献
Calderoni, Francesca; Demartin, Francesco; De Biani, Fabrizia Fabrizi; Femoni, Cristina; Iapalucci, M. Carmela; Longoni, Giuliano; Zanello, Piero
European Journal of Inorganic Chemistry, 1999 , # 4 p. 663 - 671
