反应条件
1: 3,5-dibromo-1-fluorobenzene With n-butyllithium in tetrahydrofuran; hexane; water T=-78°C; 0.75 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 1.66667 h; 3: With ammonium chloride in tetrahydrofuran; hexane; water
参考文献
Broughton, Howard Barff; Dally, Robert Dean; Durham, Timothy Barrett; Gonzalez-Garcia, Maria Rosario; Sa, Lilly; Hahn, Patric James; Henry, Kenneth James; Kohn, Todd Jonathan; McCarthy, James Ray; Shepherd, Timothy Alan; Erickson, Jon Andre; Bueno Melendo, Ana Belen
Patent: US2007/225267 A1, 2007 ;
Location in patent: Page/Page column 66-67 ;