反应条件
1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / methanol / 12 h / 20 °C 2: toluene / 2 h / Reflux 3: hydrogenchloride / 1,4-dioxane; water / 12 h / 20 °C View Scheme
参考文献
Shetty, Rupa S.; Lee, Younghee; Liu, Bin; Husain, Arifa; Joseph, Rhoda W.; Lu, Yixin; Nelson, David; Mihelcic, John; Chao, Wenchun; Moffett, Kristofer K.; Schumacher, Andreas; Flubacher, Dietmar; Stojanovic, Aleksandar; Bukhtiyarova, Marina; Williams, Ken; Lee, Kyoung-Jin; Ochman, Alexander R.; Saporito, Michael S.; Moore, William R.; Flynn, Gary A.; Dorsey, Bruce D.; Springman, Eric B.; Fujimoto, Ted; Kelly, Martha J.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 1 p. 179 - 200