5-(2,6-二氟苯基)-2H-四唑合成路线 （共 7 条）
反应条件
dicyclohexyl-carbodiimide in 1,4-dioxane T=20°C; 1 h;
参考文献
Babadzhanova; Kirij; Yagupolskii; Tyrra; Naumann
Tetrahedron, 2005 , vol. 61, # 7 p. 1813 - 1819
反应条件
triethylamine in tetrahydrofuran T=20°C; 12 h;
参考文献
Christensen, Jorn B.
Molecules, 2001 , vol. 6, # 1 p. 47 - 51
反应条件
1: SOCl2 / dimethylformamide 2: 92 percent / Et3N / tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Christensen, Jorn B.
Molecules, 2001 , vol. 6, # 1 p. 47 - 51
反应条件
in chloroform T=20°C;
参考文献
Dordea, Crenguta; Brisach, Frederic; Haddaoui, Jaouad; Arnaud-Neu, Francoise; Bolte, Michael; Casnati, Alessandro; Boehmer, Volker
Supramolecular Chemistry, 2010 , vol. 22, # 6 p. 347 - 357
反应条件
1: pyridine-2-carboxylic acid pentafluorophenyl ester With palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in toluene T=115°C; 0.166667 h; 2: 4-nitrobenzaldehdye With tert.-butylhydroperoxide in toluene 48 h; Reflux;
参考文献
Bao, Yong-Sheng; Chen, Chao-Yue; Huang, Zhi-Zhen
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8344 - 8349,6
反应条件
hydrazine in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Zhao, He; Burke Jr., Terrence R.
Tetrahedron, 1997 , vol. 53, # 12 p. 4219 - 4230
反应条件
in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Zhao, He; Burke Jr., Terrence R.
Tetrahedron, 1997 , vol. 53, # 12 p. 4219 - 4230
