3-溴-2-羟基-4,4,5,5-四甲基环戊-2-烯-1-酮合成路线 (共 2 条)
反应条件
sulfuric acid T=0°C; 24 h;
参考文献
Gill, G. Bryon; Idris, Muhammad S. Hj.; Kirollos, Kirollos S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2355 - 2366
反应条件
1: 86 percent / Br2 / CCl4 / 0.5 h / Ambient temperature 2: 82 percent / pyridine / 24 h / 0 °C 3: 83 percent / conc. H2SO4 / 24 h / 0 °C View Scheme
参考文献
Gill, G. Bryon; Idris, Muhammad S. Hj.; Kirollos, Kirollos S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2355 - 2366