3-氨基甲基吲哚-1-羧酸叔丁酯合成路线 （共 6 条）
反应条件
sodium tetrahydroborate; nickel dichloride in methanol 0.0833333 h; Ambient temperature;
参考文献
Synlett, , vol. 1997, # 3 p. 289 - 290
Tetrahedron, , vol. 54, # 14 p. 3549 - 3566
反应条件
1: 90 percent / 30percent NaOH, nBu4NBr / benzene / 0.08 h / Ambient temperature 2: 98 percent / NH2OH*HCl, Na2CO3 / ethanol; H2O / 0.08 h / 50 °C 3: 75 percent / NiCl2*6H2O, NaBH4 / methanol / 0.08 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 54, # 14 p. 3549 - 3566
反应条件
1: 98 percent / NH2OH*HCl, Na2CO3 / ethanol; H2O / 0.08 h / 50 °C 2: 75 percent / NiCl2*6H2O, NaBH4 / methanol / 0.08 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 54, # 14 p. 3549 - 3566
反应条件
1: 90 percent / 30percent NaOH, nBu4NBr / benzene / 0.08 h / Ambient temperature 2: 98 percent / NH2OH*HCl, Na2CO3 / ethanol; H2O / 0.08 h / 50 °C 3: 75 percent / NiCl2*6H2O, NaBH4 / methanol / 0.08 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 54, # 14 p. 3549 - 3566
反应条件
1: 63 percent / CaCO3 / CH2Cl2; H2O / Ambient temperature 2: 97 percent / methanol / Ambient temperature 3: 81 percent / 15-crown-5-ether / acetonitrile / 1.17 h / Ambient temperature View Scheme
参考文献
Kutschy, Peter; Dzurilla, Milan; Takasugi, Mitsuo; Toeroek, Marcel; Achbergerova, Ingrid; Homzova, Renata; Racova, Maria
Tetrahedron, 1998 , vol. 54, # 14 p. 3549 - 3566
反应条件
1: 63 percent / CaCO3 / CH2Cl2; H2O / Ambient temperature 2: 97 percent / methanol / Ambient temperature 3: 92 percent / 15-crown-5-ether, piperidine / acetonitrile / 1.42 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 54, # 14 p. 3549 - 3566
