1: With C20H24F6MnN4O6S2 in acetonitrile T=20°C; 0.05 h; Inert atmosphere; 2: With peracetic acid in acetonitrile T=20°C; 1.33333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Cheng-Xia; Wang, Shou-Feng; Kuehn, Fritz E.; Xia, Chun-Gu; Sun, Wei
Journal of Organometallic Chemistry, 2012 , vol. 715, p. 9 - 12
poly-L-leucine; dihydrogen peroxide; ammonium hydrogen carbonate; 336(R) in ethylene glycol dimethyl ether; water T=20°C; Title compound not separated from byproducts;
1: 97 percent / NAP-MgO; 4A molecular sieves / toluene / 14 h / Heating 2: TBHP; NAP-MgO; (+)-diethyl tartrate / toluene / 36 h / 25 °C View Scheme
参考文献
Choudary, Boyapati M.; Kantam, Mannepalli L.; Ranganath, Kalluri V. S.; Mahendar, Koosam; Sreedhar, Bojja
Journal of the American Chemical Society, 2004 , vol. 126, # 11 p. 3396 - 3397
1: 97 percent / NAP-MgO; 4A molecular sieves / toluene / 14 h / Heating 2: TBHP; NAP-MgO; (+)-diethyl tartrate / toluene / 36 h / 25 °C View Scheme
参考文献
Choudary, Boyapati M.; Kantam, Mannepalli L.; Ranganath, Kalluri V. S.; Mahendar, Koosam; Sreedhar, Bojja
Journal of the American Chemical Society, 2004 , vol. 126, # 11 p. 3396 - 3397
