1,10-菲咯啉1-氧化物合成路线 （共 9 条）
参考文献
Engbersen; Koudijs; Joosten; Van der Plas
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 989 - 900
反应条件
benzoyl chloride in water T=20°C; 1 h;
参考文献
Ryan, Patrick E.; Guenee, Laure; Piguet, Claude
Dalton Transactions, 2013 , vol. 42, # 31 p. 11047 - 11055
反应条件
1: benzoyl chloride / water / 1 h / 20 °C 2: water; sodium hydroxide / ethanol / |Reflux View Scheme
参考文献
Akerboom, Sebastiaan; Van Den Elshout, Jos J. M. H.; Mutikainen, Ilpo; Siegler, Maxime A.; Fu, Wen Tian; Bouwman, Elisabeth
European Journal of Inorganic Chemistry, 2013 , # 36 p. 6137 - 6146
反应条件
1: 52 percent / NaCl; POCl3 / dimethylformamide / 6 h / 100 °C 2: 56 percent / acetamide; K2CO3 / 1.5 h / 200 °C View Scheme
参考文献
Engel, Yoni; Dahan, Adi; Rozenshine-Kemelmakher, Emily; Gozin, Michael
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2318 - 2328
反应条件
sodium chloride; trichlorophosphate in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Engel, Yoni; Dahan, Adi; Rozenshine-Kemelmakher, Emily; Gozin, Michael
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2318 - 2328
反应条件
1: With tetrabutylammomium bromide in dichloromethane T=20°C; 0.166667 h; Inert atmosphereMolecular sieve; 2: With p-methylbenzenesulfonyl (tosylate) in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Wengryniuk, Sarah E.; Weickgenannt, Andreas; Reiher, Christopher; Strotman, Neil A.; Chen, Ke; Eastgate, Martin D.; Baran, Phil S.
Organic Letters, 2013 , vol. 15, # 4 p. 792 - 795
反应条件
1.1: benzoyl chloride / water / 0.42 h
2.1: sodium / 0.5 h / |Reflux
2.2: 0.5 h / 0 °C
View Scheme
参考文献
Akerboom, Sebastiaan; Van Den Elshout, Jos J. M. H.; Mutikainen, Ilpo; Siegler, Maxime A.; Fu, Wen Tian; Bouwman, Elisabeth
European Journal of Inorganic Chemistry, 2013 , # 36 p. 6137 - 6146
反应条件
HOF* CH3CN in chloroform
Oxidation;
参考文献
Rozen, Shlomo; Dayan, Sharon
Angewandte Chemie - International Edition, 1999 , vol. 38, # 23 p. 3472 - 3473
反应条件
1: benzoyl chloride / water / 1 h / 20 °C
2: water; sodium hydroxide / ethanol / |Reflux
3: thionyl chloride / 0.5 h / |Reflux
View Scheme
参考文献
Ryan, Patrick E.; Guenee, Laure; Piguet, Claude
Dalton Transactions, 2013 , vol. 42, # 31 p. 11047 - 11055
