1-甲基-1H-吲唑-5-甲腈合成路线 （共 4 条）
参考文献
Merck and Co., Inc.
Patent: US6610692 B1, 2003 ;
US 6610692 B1
反应条件
1: 91 percent / diethyl ether / 1 h / Ambient temperature 2: 75 percent / 2 h / 250 °C View Scheme
参考文献
Halley, Frank; Sava, Xavier
Synthetic Communications, 1997 , vol. 27, # 7 p. 1199 - 1207
反应条件
1: 65 percent / dimethylformamide / Heating 2: 91 percent / diethyl ether / 1 h / Ambient temperature 3: 75 percent / 2 h / 250 °C View Scheme
参考文献
Halley, Frank; Sava, Xavier
Synthetic Communications, 1997 , vol. 27, # 7 p. 1199 - 1207
反应条件
1: With diisobutyl-aluminum chloride in toluene T=-70 - -60°C; 4.33333 h; 2: With acetic acid in toluene
参考文献
GLAXO GROUP LIMITED
Patent: WO2006/759 A1, 2006 ;
Location in patent: Page/Page column 23 ;
WO 2006/000759 A1
