1-(3-二甲基氨基丙基)-3-乙基碳二亚胺合成路线 （共 7 条）
反应条件
triethylamine; p-toluenesulfonyl chloride in dichloromethane 4 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 7090
反应条件
potassium carbonate in trifluoromethylbenzene (BTF); water
参考文献
US2007/197576 A1, ;
Page/Page column 4 ;
反应条件
1: diethyl ether / 2 h / Ambient temperature 2: 60 percent / triethylamine, toluenesulfonyl chloride / CH2Cl2 / 4 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, p. 7090
反应条件
(i) Et2O, (ii) HgO, benzene; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 84, p. 4457 - 4464
反应条件
(i), (ii) TsCl; Multistep reaction;
参考文献
Tetrahedron, , vol. 31, p. 1619 - 1622
反应条件
1: in trifluoromethylbenzene (BTF) T=24 - 38°C; 2: With water; acetic acid in trifluoromethylbenzene (BTF) pH=5.0 - 5.5; 3: With potassium hydroxide in tert-butyl methyl ether; water pH=9.5 - 10.0;
参考文献
Resolution Chemicals Limited
Patent: US2007/197576 A1, 2007 ;
Location in patent: Page/Page column 4; 1 ;
反应条件
sodium sulfate in dichloromethane
参考文献
Kyriatsoulis, Apostolos; Feldmann, Susanne; Huber, Eramus; Horn, Nicole; Proff, Leopold von
Patent: US2009/93445 A1, 2009 ;
