1,3-二氯-1,1,3,3-四氟-2-苯基-丙-2-醇合成路线 (共 3 条)
反应条件
hydrogen cation in N,N,N',N',N'',N''-hexamethylphosphoric triamide decompn. in the presence of CF3CH2OH at reflux temp., 12 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 1.2, page 1 - 15
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium chloride in tetrahydrofuran
参考文献
Wheaton,G.A.; Burton,D.J.
Journal of Organic Chemistry, 1978 , vol. 43, p. 2643 - 2651
反应条件
(i) LiCl, HMPT, (ii) H2O; Multistep reaction;
参考文献
Burton,D.J.; Wheaton,G.A.
Journal of the American Chemical Society, 1974 , vol. 96, p. 6787 - 6788