O-(2-氨基乙基)-O’-[2-(叔丁氧羰基-氨基)乙基]四乙二醇合成路线 （共 9 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethanol
参考文献
Gerard, Estelle; Meulle, Aline; Feron, Olivier; Marchand-Brynaert, Jacqueline
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 586 - 590
反应条件
1: triethylamine / dichloromethane 2: sodium azide / N,N-dimethyl-formamide / 70 °C 3: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: sodium hydroxide / water; toluene / 100 °C 2: triethylamine / dichloromethane 3: sodium azide / N,N-dimethyl-formamide / 70 °C 4: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: sodium azide / N,N-dimethyl-formamide / 70 °C 2: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: ethanol 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 3: sodium hydroxide / water; toluene / 100 °C 4: triethylamine / dichloromethane 5: sodium azide / N,N-dimethyl-formamide / 70 °C 6: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: sodium azide; sodium iodide / water / 96 h / 50 °C 2: palladium 10 on activated carbon; hydrogen / ethanol 3: ethanol 4: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 5: sodium hydroxide / water; toluene / 100 °C 6: triethylamine / dichloromethane 7: sodium azide / N,N-dimethyl-formamide / 70 °C 8: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: ethanol 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 3: sodium hydroxide / water; toluene / 100 °C 4: triethylamine / dichloromethane 5: sodium azide / N,N-dimethyl-formamide / 70 °C 6: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: palladium 10 on activated carbon; hydrogen / ethanol 2: ethanol 3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 4: sodium hydroxide / water; toluene / 100 °C 5: triethylamine / dichloromethane 6: sodium azide / N,N-dimethyl-formamide / 70 °C 7: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 4 h 2: sodium hydroxide / water; toluene / 100 °C 3: triethylamine / dichloromethane 4: sodium azide / N,N-dimethyl-formamide / 70 °C 5: palladium 10 on activated carbon; hydrogen / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 586 - 590
