N,N-二甲基-2-苯基乙酰胺合成路线 （共 47 条）
反应条件
dysprosium
T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Chen, Weifeng; Li, Kebin; Hu, Ziqiang; Wang, Liliang; Lai, Guoqiao; Li, Zhifang
Organometallics, 2011 , vol. 30, # 7 p. 2026 - 2030
反应条件
in benzene
12 h; Heating;
参考文献
Levin, Jeremy I.; Turos, Edward; Weinreb, Steven M.
Synthetic Communications, 1982 , vol. 12, # 13 p. 989 - 994
反应条件
KNH2 in ammonia
1.5 h; Irradiation;
参考文献
Palacios, S. M.; Asis, S. E.; Rossi, R. A.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, # 1 p. 111 - 116
反应条件
in tetrahydrofuran; pentane
Ambient temperature;
参考文献
Riviere-Baudet; Morere; Dias
Tetrahedron Letters, 1992 , vol. 33, # 43 p. 6453 - 6456
反应条件
1: 48 percent / triethylamine / tetrahydrofuran; diethyl ether / Heating
2: Zn / acetic acid / 0.5 h / Heating
View Scheme
参考文献
Zvilichovsky, Gury
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 465 - 470
反应条件
potassium permanganate; N-benzyl-N,N,N-trimethyl-ammonium chloride in dichloromethane
3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Markgraf, J. Hodge; Sangani, Poorab K.; Finkelstein, Manuel
Synthetic Communications, 1997 , vol. 27, # 7 p. 1285 - 1290
反应条件
1: 89 percent / C2H5MgBr / diethyl ether / 1. 2.5 h, reflux; 2. 3 h, 20 deg C
2: 74 percent / 4-Dimethylaminopyridine / tetrahydrofuran / 8 h / 60 °C
View Scheme
参考文献
Tikhomirov, D. A.; Eremeev, A. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 1 p. 30 - 34
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 1 p. 39 - 43
参考文献
Kirsanow; Solotow
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1166,1168; engl. Ausg. S. 1273, 1275
反应条件
oxalyl dichloride; N,N-dimethyl-formamide
1.) CH2Cl2, RT, 4 h; Multistep reaction;
参考文献
Yardley; Morris Husbands; Stack; Butch; Bicksler; Moyer; Muth; Andree; Fletcher III; James; Sielecki
Journal of Medicinal Chemistry, 1990 , vol. 33, # 10 p. 2899 - 2905
反应条件
1: SOCl2
View Scheme
参考文献
Lee; Mayer; Wiegrebe; Lauber; Schlunegger
Archiv der Pharmazie, 1988 , vol. 321, # 5 p. 265 - 272
